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2 article(s) from Belo, Dulce

Synthesis and characterization of the cyanobenzene-ethylenedithio-TTF donor

Sandrina Oliveira,
Dulce Belo,
Isabel C. Santos,
Sandra Rabaça and
Manuel Almeida

Beilstein J. Org. Chem. 2015, 11, 951–956, doi:10.3762/bjoc.11.106

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Scheme 1: Synthesis of cyanobenzene-ethylenedithio-tetrathiafulvalene (CNB-EDT-TTF) 3.

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Figure 1: ORTEP diagrams of compound 3 drawn at 30% probability level with the atomic numbering scheme.

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Figure 2: Crystal structure of compound 3 viewed along the b axis.

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Figure 3: View of three neighbouring molecular stacks in 3.

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Figure 4: Cyclic voltammogram of 3.

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Letter

Published 03 Jun 2015

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TTFs nonsymmetrically fused with alkylthiophenic moieties

Rafaela A. L. Silva,
Bruno J. C. Vieira,
Marta M. Andrade,
Isabel C. Santos,
Sandra Rabaça,
Dulce Belo and
Manuel Almeida

Beilstein J. Org. Chem. 2015, 11, 628–637, doi:10.3762/bjoc.11.71

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Scheme 1: Molecular diagrams of α-tbtdt (1) and α-mtdt (2), and related TTF-type donors.

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Scheme 2: Synthetic route for compounds 1 and 2.

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Figure 1: Cyclic voltammogram of α-tbtdt (1) and α-mtdt (2) (10⁻³ M) in dichloromethane versus Ag/AgNO₃, with ...

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Figure 2: ORTEP view and atomic numbering scheme of I with thermal ellipsoids at 50% probability level.

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Figure 3: Molecular herringbone bi-chains in the crystal structure of I: a) view along the molecular planes a...

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Figure 4: Crystal structure of I a) view along the b axis, b) Partial view of one layer of bi-chains in the a...

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Figure 5: ORTEP views and atomic numbering scheme of α-tbtdt (1) with thermal ellipsoids at 50% probability l...

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Figure 6: Crystal structure of 1 a) view along the b axis; b) Partial view of one chain in the b,c plane (top...

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Figure 7: ORTEP views and atomic numbering scheme of a) (α-mtdt)⁺ and b) [Au(mnt)₂ ]⁻ in compound 3, with the...

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Figure 8: Crystal structure of 3 a) viewed along the b axis and b) partial view showing the alternated A–D–A–...

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Figure 9: Detail of the crystal structure of 3 showing the short contacts between stacks.

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Full Research Paper

Published 05 May 2015

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